SULFATES - RECHERCHE
COEI-2-SULFAT Search for sulphates
In a 160 16 mm test tube, place the volume prescribed of the solution obtained by the means indicated in each monography; add 1 ml of diluted hydrochloric acid (R); adjust to 20 ml with water and add 2 ml of barium chloride solution at 10% (R).
SODIUM - DOSAGE PAR SAA
COEI-2-SODIUM Determination of sodium by absorption atomic spectrometry
- Principle
The sodium is determined after mineralisation by dry process by atomic absorption spectrometry.
The addition of a spectral buffer (cesium chloride) to avoid ionisation of sodium is necessary.
SELENIUM - DOSAGE PAR SAA
COEI-2-SELENI Determination of selenium by atomic absorption spectrometry
- Principle
After mineralisation of the sample by wet process, the selenium is determined by atomic absorption spectrometry without flame (electro-thermal atomisation in the graphite oven).
SACCHAROSE - SUCRE DE RAISIN - DOSAGE
COEI-2-SUCSAC Grape sugar: Determination of saccharose by HPLC
- Principle
The samples diluted or put in solution are analysed by high performance liquid chromatography: Separation on column of grafted silica NH2 and detection using a differential refractometer.
POTASSIUM - DOSAGE PAR SAA
COEI-2-POTASS Determination of potassium by atomic absorption spectrometry
- Principle
The potassium is determined by mineralisation by dry process by atomic absorption spectrometry.
The addition of a spectral buffer (cesium chloride) to avoid the ionisation of the potassium is necessary.
PLOMB - DOSAGE PAR SAA
COEI-2-PLOMB Determination of lead by atomic absorption spectrometry
- Principle
After mineralisation of the sample in an acid medium, the lead is determined by spectrometry without flame (electro-thermal atomisation).
NICKEL - DOSAGE PAR SAA
COEI-2-NICKEL Determination of nickel by atomic absorption spectrometry
- Principle
The nickel is directly determined by atomic absorption spectrometry without flame (electro-thermal atomisation).
METHODES DE MINERALISATION AVANT DOSAGE PAR SAA
COEI-2-MINERA Mineralisation methods of samples before determination by atomic absorption spectrometry
- Mineralisation by dry process
Method applicable for determining the following elements: calcium, magnesium, sodium, iron, copper, zinc.
METAUX LOURDS - RECHERCHE
COEI-2-METAUX Search for heavy metals
- Principle of the method
Heavy metals react with the thiol function to form sulphurs. The coloration that results is compared to a standard.
MERCURE - DOSAGE
COEI-2-MERCUR Determination of mercury by the generation of vapour and atomic fluorescence spectrometry
- Field of application
This method is applied to the analysis of mercury in oenological products in the concentration range of 0 to 10 μg/l.
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